水提醇沉法和醇提水沉法有什么区别

2025-03-10 00:54:59
推荐回答(2个)
回答1:

  水提醇沉法(水醇法)系指在中药水提浓缩液中,加入乙醇使达不同含醇量,某些药物成分在醇溶液中
  溶解度降低析出沉淀,
  固液分离后使水提液得以精制的方法。
  一般操作过程是:
  将中药水提液浓缩至
  1
  ︰
  1
  ~
  1
  ︰
  2
  (
  ml
  ︰
  g
  )
  ,药液放冷后,边搅拌边缓慢加入乙醇使达规定含醇量,密闭冷藏
  24
  ~
  48h
  ,滤过,滤液回
  收乙醇,得到精制液。操作时应注意以下问题:①药液应适当浓缩,以减少乙醇用量。但应控制浓缩程度,
  若过浓,有效成分易包裹于沉淀中而造成损失。②浓缩的药液冷却后方可加入乙醇,以免乙醇受热挥发损
  失。③选择适宜的醇沉浓度。一般药液中含醇量达
  50
  %~
  60
  %可除去淀粉等杂质,含醇量达
  75
  %以上大部
  分杂质均可沉淀除去。④慢加快搅。应快速搅动药液,缓缓加入乙醇,以避免局部醇浓度过高造成有效成
  分被包裹损失。⑤密闭冷藏。可防止乙醇挥发,促进析出沉淀的沉降,便于滤过操作。⑥洗涤沉淀。沉淀
  采用乙醇(浓度与药液中的乙醇浓度相同)洗涤可减少有效成分在沉淀中的包裹损失。
  
  水提醇沉法(水醇法)系指在中药水提浓缩液中,加入乙醇使达不同含醇量,
  某些药物成分在醇溶液中溶解度降低析出沉淀
  ,固液分离后使水提液得以精制
  的方法。一般操作过程是:将中药水提液浓缩至
  1
  ︰
  1
  ~
  1
  ︰
  2
  (
  ml
  ︰
  g
  ),药液放
  冷后,边搅拌边缓慢加入乙醇使达规定含醇量,密闭冷藏
  24
  ~
  48h
  ,滤过,滤液
  回收乙醇,得到精制液。操作时应注意以下问题:
  ①
  药液应适当浓缩,以减少
  乙醇用量。但应控制浓缩程度,若过浓,有效成分易包裹于沉淀中而造成损失。
  ②
  浓缩的药液冷却后方可加入乙醇,以免乙醇受热挥发损失。
  ③
  选择适宜的醇
  沉浓度。一般药液中含醇量达
  50
  %~
  60
  %可除去淀粉等杂质,含醇量达
  75
  %以
  上大部分杂质均可沉淀除去。
  ④
  慢加快搅。应快速搅动药液,缓缓加入乙醇,
  以避免局部醇浓度过高造成有效成分被包裹损失。
  ⑤
  密闭冷藏。可防止乙醇挥
  发,促进析出沉淀的沉降,便于滤过操作。
  ⑥
  洗涤沉淀。沉淀采用乙醇(浓度
  与药液中的乙醇浓度相同)洗涤可减少有效成分在沉淀中的包裹损失。
  
  醇提水沉法(醇水法)系指先以适宜浓度的乙醇提取药材成分,将提取液
  回收乙醇后,加适量水搅匀,静置冷藏一定时间,沉淀完全后滤除的方法。药
  材用乙醇为溶剂提取,可避免淀粉、蛋白质、黏液质等成分的浸出,加水处理
  后可除去醇提液中树脂、脂溶性色素等杂质。应用此方法要慎重,避免醇溶性
  有效成分因水溶性差而被一起沉淀除去。

回答2:

水提醇沉法系指处方中药材加水煎煮,既提取出有效成分,如:生物碱盐、甙类、有机酸类、氨基酸、多糖类等;同时也提出一些水溶性杂质,如:淀粉、蛋白质、粘液质、鞣质、色素、无机盐等。若往水煎液中加入适量乙醇,可以改变其溶解性能而将杂质部分或全部除去。当乙醇浓度达到60%~70%时,除鞣质、树脂等外,其他杂质已基本上沉淀而除去。如果分2~3次加入乙醇,浓度又逐步提高,最终达到75%~80%,则除去杂质的效果更好。
醇提水沉法系指将中药原料用一定浓度的乙醇用渗漉法、回流法提取,即可提取出生物碱及其盐、甙类、挥发油及有机酸类等;虽然多糖类、蛋白质、淀粉等无效成分不易溶出,但树脂、油脂、色素等杂质却仍可提出。为此,醇提取液经回收乙醇后,再加水处理,并冷藏一定时间,可使杂质沉淀而除去。40%~50%的乙醇可提取强心甙、鞣质、蒽醌及其甙、苦味质等;60%~70%乙醇可提取甙类;更高浓度乙醇则可用于生物碱、挥发油、树脂和叶绿素的提取。

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